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Acetic Acid Glacial Preparation: Dissolve an appropriate amount of sodium hydroxide in water to prepare a saturated solution. After cooling, store it in a polyethylene plastic bottle and let it stand for several days until clear. Take 56 mL of the clarified saturated sodium hydroxide solution and dilute to 1000 mL with freshly boiled and cooled water. Mix well.Acetic Acid Glacial.